High shear rotor-stator mixers are widely used in process industries including the
manufacture of many food, cosmetic, health care products, fine chemicals and
pharmaceuticals. Rotor-stator devices provide a focussed delivery of energy, power & shear
to accelerate physical processes such as mixing, dissolution, emulsification and deagglomeration.
To reliably scale-up these devices we need to understand the relationship
between rotor speed and flow rate and the energy dissipated by these devices. In-line rotor
stator mixers differ from in-tank versions because the flow is usually controlled
independently of the rotor speed. For in-tank devices the turbulent power can usually be
adequately described by single impeller type power number1. For an in-line rotor-stator
mixer it is found that the power transmitted by the rotor drops in proportion to decreased
flow rate and a single power number is not adequate. Kowalski2 and Baldyga et al.3
proposed that the power draw of a rotor-stator mixer can be described by the expression;
P= POZ ρ N3 D5 + k1 M N2 D2 (1)
This expression consists of two main elements. Firstly a term reflecting the power required
to rotate the shaft in response to the resistance of the liquid in the process chamber where ρ
is density (kg/m3), N is rotor speed (rps) and D is rotor diameter (m). Secondly a term for the
centrifugal energy given to the fluid which is then convected away by the mass flow rate, M
(kg/s). The two constants POZ and k1 are normally obtained from a multi-linear regression a
large matrix of experiments covering a wide range of flow rates and rotor speeds 4.
In the experiments described herein, it has been found that good estimates of the constants
can be obtained using a simplified set of trials. In Method 1 we note that there are two sets
of conditions under which constant turbulent power numbers are obtained as follows.
• When the outlet valve is closed, so we have zero flow, then the power is a minimum
given by P = POZ ρ N3 D5 with the characteristic power number POZ
• When the valve is fully open and the rotor-stator device acts as the sole pumping agent
then the flow rate is proportional to the rotor speed (figure 1) with M = ρ k2ND3. Power
draw is a maximum given by Pmax = POU ρ N3 D5 which can also be expressed as:
POZ ρ N3 D5 + (POU – POZ)ρN3 D5 with the characteristic power number POU
Substituting for M in eq 1 & rearranging gives Pmax = (POZ + k1 k2) ρ N3 D5 = POU ρ N3 D5 (2)
which in turn yields k1 = (POU – POZ) / k2 (3)
Figure 2 presents an example of the values of PO determined for these two extreme cases
and illustrates that the values are constant for all rotor speed and figure 3 presents the
comparison of measured and predicted power draw for a range of conditions.
In Method 2 we consider the example of a fixed speed device where flow rate can be varied
by means of a backpressure valve. In this case the power is a linear function of the flow rate
(fig 4) where the intercept is given by POZ ρ N3 D5 and the gradient by k1 N2 D2 and thus POZ
and k1 can be determined. This method also has the advantage of being suitable with power
determined from a heat balance because it does not explicitly require measurement at zero
flow rate (this is possible with the torque measurement used above). However at low rotor
speeds and high flow rates the temperature rise is small the heat balance is subject to
significant errors although the accuracy was improved by lagging the equipment and careful
calibration of the temperature probes. Table 1 presents the values of the constants
determined by the two approaches for an example arrangement of rotor and stator. In the
presentation we will present results for other arrangements complete with statistical analysis.