FLOW AND MIXING CHARACTERISTICS OF σ-TYPE PLATE STATIC MIXER WITH SPLITTING AND INVERSE RECOMBINATION

A new type static mixer composed of σ-shaped elementmultipase
was developed, in which multilamination of fluid layers
proceeds through systematic splitting and inverse
recombination. The number of elements required for
complete mixing, n, was measured by conducting the
decolourising reaction of iodine with sodium thiosulfate
for various total flow rates of two fluids to be mixed. n
increased with Re when Re is less than 10, but it decreased
with Re at larger Re. When Re exceeds this critical value,
CFD analysis shows that a larger deformation and stretch
of the fluid interface take place due to the bending and
winding channel structure of σ-shaped element as Re
increases. This flow behaviour accelerates mixing rate,
resulting in the considerable decrease in the number of
elements for complete mixing. In addition, an analysis for
Figure
residence time distribution of fluid particles demonstrates
that the flow in the mixer approaches the plug flow with
increasing the Reynolds number and the number ofmultipase2
elements.
NOMENCLATURE
a largest width of channel of mixing element
b depth of channel of mixing element
n number of mixing elements for complete mixing
Re Reynolds number = ρuava/μ
uav cross-sectional average velocity = Q/ab
Q total flow rate of two fluids fed to mixer
MIXER STRUCTURE
Figure 1 shows channel geometry of a unit element of σ-
type plate static mixer (Hirata, 2006), in which the dotted
circles represent the cross-sections of inlet and outlet for
the fluids to be mixed. Channels with rectangular crosssection
were grooved in a plate to conform this geometry
and each grooved element was aligned in a row. A
packing sheet or plate with circular holes is sandwiched
by two plates with a row of unit elements prepared in this
way, to one of which a Y-shaped channel was connected
for introducing two fluids to be mixed as shown in Figure
2. Each hole of the sandwiched sheet or plate serves as a
channel connecting the outlet of a unit element on a plated
to the inlet of the following unit element on the other plate.
In this way channels for mixing fluids can be constructed.
We call this type of mixer σ-type plate static mixer since
the shape of the unit element resembles σ in Greek
character.

this way, static mixing with splitting and inverse
recombination progresses in the mixer.
VISUALIZATION OF MIXING PTROGRESS
Mixing progress was visualized by using the decolourising
reaction of iodine with sodium thiosulphate. An example
of the visualized images is shown in Fig.3, which were
taken at Re=1.2 using the square channel with a=b=3mm.
At low Reynolds numbers, the static mixing progresses
identically by splitting and inverse recombination as
shown in the figure. As the Reynolds number increases,
mixing progress deviates from the ideal static mixing
because of the secondary flows generated in the threedimensionally
bent portions in the mixer. The occurrence
of secondary flows has been confirmed by CFD
calculation.
NUMBER OF ELEMENTS REQUIRED FOR
COMPLETE MIXING
The numbers of elements required for completing the
decolourising reaction, n, which were obtained for a
square channel with a=b=1mm, is plotted against
Reynolds number in Fig. 4. n increases with Reynolds
number at Re < 10. This is due to that the molecular
diffusion is limited to narrow regions adjacent to the
interface of two liquids because the residence time in the
element is decreased with increasing the flow velocity. At
larger Reynolds number, n decreases with Re. The
decrease in n is mainly caused by the secondary flows
generated in the three-dimensionally bent portions in the
mixer. At Reynolds number greater than 102, the number
of elements required for complete mixing is less than 10.
RESIDENCE TIME DISTRIBUTION
F-curves in a unit element are shown for various Reynolds
numbers in Fig. 5. Using the three-dimensional velocity
data obtained by CFD calculation, F-curves were obtained
by tracking 105 fluid particles that were uniformly
distributed on the mid-plane of the interconnecting
circular channel at a time. Although this curve does not
represent the normal F-curve obtained by a step change in
concentration, reactor performance of σ-type mixer may
be discussed based on it. As shown in the figure, F-curve
for fluid particles, which are sharp compared with that in
the laminar pipe flow, approach the distribution of plug
flow as Reynolds number increases. It has also been
confirmed that the flow in the mixer tends to approach the
uniform residence time distribution with increasing the
number of mixing elements. You can even create solid metal hitch covers using this method.

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